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Gewählte Publikation:

Malachova, A; Stranska, M; Vaclavikova, M; Elliott, CT; Black, C; Meneely, J; Hajlova, J; Ezekiel, CN; Schuhmacher, R; Krska, R.
(2018): Advanced LC-MS-based methods to study the co-occurrence and metabolization of multiple mycotoxins in cereals and cereal-based food
ANAL BIOANAL CHEM. 2018; 410(3): 801-825. FullText FullText_BOKU

Liquid chromatography (LC) coupled with mass spectrometry (MS) is widely used for the determination of mycotoxins in cereals and cereal-based products. In addition to the regulated mycotoxins, for which official control is required, LC-MS is often used for the screening of a large range of mycotoxins and/or for the identification and characterization of novel metabolites. This review provides insight into the LC-MS methods used for the determination of co-occurring mycotoxins with special emphasis on multiple-analyte applications. The first part of the review is focused on targeted LC-MS approaches using cleanup methods such as solid-phase extraction and immunoaffinity chromatography, as well as on methods based on minimum cleanup (quick, easy, cheap, effective, rugged, and safe; QuEChERS) and dilute and shoot. The second part of the review deals with the untargeted determination of mycotoxins by LC coupled with high-resolution MS, which includes also metabolomics techniques to study the fate of mycotoxins in plants.
Autor*innen der BOKU Wien:
Krska Rudolf
Malachova Alexandra
Schuhmacher Rainer
Vaclavikova Marta

Find related publications in this database (Keywords)
Fungal secondary metabolites
Liquid chromatography-tandem mass spectrometry
Liquid chromatography-high-resolution mass spectrometry

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